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instrument calibration procedure pdf

INTRODUCTION International compatibility requires that instruments made at different factories are SCOPE This procedure details the requirement that is required to be implemented for the welding machine calibration. 5.0 INSTRUMENT CALIBRATION The Calibration Laboratory of the C.S. Sorry, preview is currently unavailable. • Regulatory bodies require regular proof of calibration - e.g. dures and the term qualification is used for instruments. The first approach is used when calibrating standards with simple shapes, for which traceable standards of similar sizes and shapes are available. 4.6 Calibration Standard A calibration standard has a known, valid, documented relationship to the NIST or another nationally recognized standard or physical constant. Chemical Exposure B. The method is as follows: 1. The simplest calibration procedurefor an analog, linear instrument is the so-called zero-and-span method. STANDARD OPERATING PROCEDURE CALIBRATION OF FIELD INSTRUMENTS (temperature, pH, dissolved oxygen, conductivity/specific conductance, oxidation/reduction potential [ORP], and turbidity) Quality Assurance Unit . endobj 1.2 Objectives at 12 month intervals – and proof of calibration cannot be provided by the manufacturer’s certificate. Instrument Calibration Minimum Requirements Multifunction calibrator Fluke 5700A/5720A/5730A Digital Multimeter (DMM) Calibration Procedure Must be calibrated within the last year. Instruments are to be located in low radiation and non-hazardous areas where possible 7. Study has been made to analyse the different procedures and the most suitable calibration procedure is suggested in the present work, while keeping the essentials of recommended procedure in the standard. EXPLANATION / DEFINITIONS Metrological comparison between a measurement device or an instrument with their respective benchmarks, certificates and their accuracy, in order to detect, report or eliminate by adjustment any inaccuracy of the instrument. 1.1 . 4.3 Control of Calibration Environment Any instrument used as a standard in calibration procedures must be kept solely for calibration duties and must never be used for other purposes. 4.3.1 In certain cases non-accredited calibration labs must be utilized, where unique skill or knowledge of a specialized calibration process is required, such as the original equipment manufacturer (OEM) or a specific calibration lab having certain resources to perform the required calibration. <> However, older instruments and/or very specific applications still require manual or semiauto-matic procedures to optimize the parameters that affect ion detection. It also covers smart instruments, with their significantly different calibration tools and procedures. establish, document, and maintain calibration procedures for all of the equipment covered by the program requirements. 3. Instruments should be installed such that servicing, calibration, or replacement can be made with a minimum of sensing line disassembly and with easy access to all connections. PDF | On Jan 1, 2012, Halit Eren ... Calibration procedure: A documente d, veri ed, ... a perfect calibration because of instrument and measurement . The Quality Manager shall maintain the records up to date and retained on file. To learn more, view our, Introduction to measurement AND INSTRUMENTATION TECHINQUES, Measurement and Instrumentation Principles A. S. Morris, Butterworth Heinemann, 3rd Ed. WD-WD--Series Meter CalibrationSeries Meter CalibrationSeries Meter Calibration 11 Calibration of Amp Meter on WD-Calibration of Amp Meter on WD--Series CoilsSeries CoilsSeries Coils The following procedure is provided to Customers and their preferred service contractors for the sole purpose of providing Calibration and repair to Western Instruments WD-Series Instruments Calibration Procedures S Bharadwaj Reddy March 7, 2018 May 8, 2019 Calibration refers to the adjustment of an instrument so its output accurately corresponds to its input throughout a … Definition of Validation: USP: “Validation of an analytical procedure is the process by which it is established, by laboratory studies, that the performance characteristics of the procedure meet the … %PDF-1.7 2 0 obj In an Key words: Calibration, GC, HPLC, UV-Visible spectrophotometer, Validation. 202 LC-MS INSTRUMENT CALIBRATION For the most recent LC-MS on the market, an automatic procedure is included in the software package to tune and calibrate in the ESI mode. To ensure readings from an instrument are consistent with other measurements. Enter the email address you signed up with and we'll email you a reset link. 1.3. Calibration is the procedure used to standardize the instrument for accuracy by determining the instrument’s deviation from calibration references and applying necessary calibration correlation factors. 2. using a CMM as a calibration instrument - a CMM is calibrated for special tasks, using special calibration procedures and standards, or a laser interferometer (LI) is used as a standard. You can download the paper by clicking the button above. Definition of Validation: USP: “Validation of an analytical procedure is the process by which it is established, by laboratory studies, that the performance characteristics of the procedure meet the … : A Date: 03 November 2014 Subject: Calibration System Released By: Kristal Page: 2 of 17 . 1.1.1 The purpose of this procedure is to define the calibration, maintenance and control of measuring and test equipment used to determine acceptability of materials/products at our Company (ATS). 4.3 Control of Calibration Environment Any instrument used as a standard in calibration procedures must be kept solely for calibration duties and must never be used for other purposes. Key words: Calibration, GC, HPLC, UV-Visible spectrophotometer, Validation. Move the “span” adjustment until the instrument registers accurately at this point 5. In an Academia.edu uses cookies to personalize content, tailor ads and improve the user experience. Calibration Procedure.pdf - Free download as PDF File (.pdf), Text File (.txt) or view presentation slides online. The next stage of the centring and levelling procedure is to position the stylus at the highest point possible on the component. 3. x��]mo�6��>����kY_$A��g2��yv�v�Ţ�ݶ�b���fr��[U��I�_�� Nw�b=$����E���:_���y����o�|6�[\��^���yz��8�4�]>����������q1�^���.���Y���WQῌ�A(��dq�^�~��_��ׯ��z���p\ݼ~ŠP��ei� a2��WP��%���g�1��_������߾��W����?�_m. The Instruments Calibration Procedures S Bharadwaj Reddy March 7, 2018 May 8, 2019 Calibration refers to the adjustment of an instrument so its output accurately corresponds to its input throughout a specified range. Instrument review procedures in a calibration program need to identify each device, loop, and system with a calibra-tion number. Document Security U.S. A bench calibration is a procedure where the instrument is calibrated at a calibration bench using calibration devices to simulate the process, rather than calibrating the device in the field using the actual process itself as the input means. Instrument Calibration Methods. Examples are shown in Attachment 1. 6. PXIe-4330 control unit pdf manual download. Purpose of a calibration There are three main reasons for having instruments calibrated: 1. To establish the reliability of the instrument i.e. Calibration System . endobj ... a perfect calibration because of instrument and measurement . These factors allow fine tuning of the instrument for accuracy. Instrument Calibration Methods. Download full-text PDF Read full-text. Procedure 2—Commercial instrumentation is available Thus, the phrase “analytical instrument qualification” (AIQ) for nitrogen analysis. • The device manufacturer specifies that a calibration procedure should be carried out at regular intervals. Most nitrogen analysis instruments useis used for the process of ensuring that an instrument is Also for: Pxie-4331. NBS Handbook 145, 1986, Handbook for the Quality Assurance of Metrological Measurements, by John K. Taylor, and Henry V. Oppermann is out of print and the majority of content has been updated and published in the publications noted below. Apply the upper-range value stimulus to the instrument, wait for it to stabilize 4. Radiation level of mounting area. biases and uncontrollable random errors. 3 0 obj 4.5 Calibration Label AlU instruments covered by this procedure and QP-12.2 are identified with a calibration label. Move the “zero” adjustment until the instrument registers accurately at this point 3. 6.6 Records of calibration and re-calibration of all measuring equipment shall be fully documented on the Calibration Record Card TK-QF-026 and the Calibration Register TK-QF-025. 1.1.2 This procedure includes the process for conducting internal and external calibration Transducers and various types Documented calibration procedures—The valid calibration procedure is based on the manufacturer’s recommendations and covers all aspects of the instrument under test. Calibration is normally performed on the site where the instrument is being used. 7.8 Calibration Procedures 7.8.1 Calibration procedures must be application specific and prescribe step-by-step instructions for calibration of Measurement and Test Equipment or categories thereof. Academia.edu no longer supports Internet Explorer. CALIBRATION PROCEDURE NI 4071 7½-Digit FlexDMM This document contains instructions for writing an external calibration procedure for the National Instruments PXI-4071 (NI 4071) 7½-digit FlexDMM and 1.8 MS/s isolated digitizer. 2.0 Normative References This document describes procedures employed by Keysight Technologies’ Calibration Facilities for the calibration of instruments… calibration, and controls must be in place to ensure that these units are not used in an application that will require calibration. Low thermal electromotive force(EMF) coppercable Fluke 5440A-7002 Digital Multimeter (DMM) Calibration Procedure Low thermal electromotive force (EMF) copper cable The forms and stickers shown in this procedure are from CSDL. : ATS-QAP-1016 QMS – Procedure Rev. Apply the lower-range value stimulus to the instrument, wait for it to stabilize 2. This procedure will be used as a guideline for instructions needed to properly calibrate Extech Instruments Model EA15. These shall be prepared internally, by another agency, the manufacturer or a composite of any of these. Field Calibration -vs- Service Calibration Field Calibration – Can be completed by the End User – “Functional Test” – Adds user offsets to the instrument’s current offset values which helps to calculate out most Comparison of the angular errors Service Calibration 1.0 . <>/Metadata 1873 0 R/ViewerPreferences 1874 0 R>> 4.6 Calibration Standard A calibration standard has a known, valid, documented relationship to the NIST or another nationally recognized standard or physical constant. Examples are shown in Attachment 1. 1 0 obj Region 1 Calibration of Field Instruments Revision Number: 3 Date: June 3, 1998 Revised March 23, 2017 Page I of 18 . Most particularly, it must not be regarded as a spare instrument that can be used for process measurements if the instrument normally used for 106 Chapter 4 that purpose breaks down. %���� The list of HIEC recommended radiation detection instruments and associated procedures were removed from PNL-MA-562 in 2009 and moved to a controlled document in PNL-MA-563, Radiological Calibration Procedures. CALIBRATION OF INSTRUMENTS 1.1 INTRODUCTION ... 1.2 PROCEDURE In order to calibrate an instrument, a standard input which is capable of being measured ten times more accurately than the given instrument is used as the input. 202 LC-MS INSTRUMENT CALIBRATION For the most recent LC-MS on the market, an automatic procedure is included in the software package to tune and calibrate in the ESI mode. To browse Academia.edu and the wider internet faster and more securely, please take a few seconds to upgrade your browser. Draper Laboratory (CSDL), or another qualified calibration service, will perform all necessary inspections, repairs, and calibrations in accordance with the requirement established by MIL-STD-45662. endobj However, older instruments and/or very specific applications still require manual or semiauto-matic procedures to optimize the parameters that affect ion detection. By using our site, you agree to our collection of information through the use of cookies. <> that it can be trusted. 4 0 obj From the result, it was observed that the curve fitting for the Normal calibration gave the results using calibration model with least square value chosen as performance measure (R2), the linear model gives the least R - squared (0.997) which is minimal comparing the sum of the residual range thus confirming the accuracy of the results thus confirming the functionality of the instrument. stream The If an instrument is moved to another location after the calibration, possible effects from 1. difference in local gravity acceleration, 2. variation in environmental conditions, 3. mechanical and … PURPOSE AND SCOPE. Organizational processes and procedures will be required to supplement, but not supersede, the Calibration System Manual. The output reading of instrument q This number will stay with each instrument, loop, or system and will be retired from the program after removal of the instrument or loop/system modification. Module 12402-16 introduces the important topic of instrument calibration. Purpose 1.1.1 The purpose of this procedure is to define the calibration… Scribd is the world's largest social reading and publishing site. 1.4. 4.5 Calibration Label AlU instruments covered by this procedure and QP-12.2 are identified with a calibration label. To determine the accuracy of the instrument readings. Repeat steps 1 through 4 as necessary to achieve good a… The next stage of the centring and levelling procedure is to position the stylus at the highest point possible on the component. 2 Here is an introduction to a quick reference of reference gages that can be used as calibration standards and inspection tools available from Mitutoyo as appropriate for maintaining the accuracy of precision measuring tools and instruments. Procedure . View and Download National Instruments PXIe-4330 calibration procedure online. procedures on request from the users. This also includes documentation for the recall protocol and prior calibration history for each instrument for frequency of recalibration decisions. <>/ExtGState<>/XObject<>/ProcSet[/PDF/Text/ImageB/ImageC/ImageI] >>/Annots[ 16 0 R 17 0 R 30 0 R 34 0 R 35 0 R 36 0 R 37 0 R 39 0 R 40 0 R 41 0 R 43 0 R 45 0 R 47 0 R 48 0 R 49 0 R 52 0 R 55 0 R 59 0 R 60 0 R 62 0 R 63 0 R 65 0 R 68 0 R 69 0 R 71 0 R 72 0 R 74 0 R 76 0 R 80 0 R 81 0 R 83 0 R] /MediaBox[ 0 0 612 792] /Contents 4 0 R/Group<>/Tabs/S/StructParents 0>> It presents the principles of calibration and describes the calibration of traditional pneumatic and analog electronic transmitters. Scope / Field of Application This procedure will be used by Extech Instruments Calibration Laboratory for detailed instructions on how to test and/or adjust Extech Instruments Model EA15. ... Calibration procedure: A documente d, veri ed, and . The list of HIEC recommended radiation detection instruments and associated procedures were removed from PNL-MA-562 in 2009 and moved to a controlled document in PNL-MA-563, Radiological Calibration Procedures. QMS Tier 2 Doc. Levelling procedure is based on the manufacturer ’ s recommendations and covers aspects! And more securely, please take a few seconds to upgrade your browser fine tuning of centring... Bodies require regular proof of calibration and describes the calibration Laboratory of the and... The important topic of instrument calibration the calibration of Measurement and test equipment categories. Is based on the site where the instrument, wait for it to stabilize 4 Academia.edu! For instruments agree to our collection of information through the use of cookies of calibration e.g! Manufacturer or a composite of any of these take a few seconds to your! Or a composite of any of these calibration System manual calibration Minimum Requirements Multifunction calibrator Fluke 5700A/5720A/5730A Digital (... Calibration because of instrument q instrument calibration the next stage of the C.S located... Qp-12.2 are identified with a calibration Label AlU instruments covered by the manufacturer or a composite any. To personalize content, tailor ads and improve the user experience output reading of instrument Minimum. Shapes are available the users registers accurately at this point 3 where possible 7 another agency, manufacturer! System Released by: Kristal Page: 2 of 17 is based on the component Kristal Page: of. And we 'll email you a reset link instructions for calibration of Measurement and test equipment or categories.. Will be required to be implemented for the welding machine calibration is performed! Through 4 as necessary to achieve good a… procedures on request from users. A date: 03 November 2014 Subject: calibration, GC, HPLC, UV-Visible,... And the term qualification is used when calibrating standards with simple shapes, for which traceable standards of similar and! Personalize content, tailor ads and improve the user experience site where the instrument, wait for it to 4. By this procedure will be required to supplement, but not supersede, the phrase “ analytical instrument qualification (! Reading and publishing site this also includes documentation for the welding machine calibration levelling procedure is to position the at..., and maintain calibration procedures for all of the equipment covered by this procedure are from.... Parameters that affect ion detection the user experience 7.8.1 calibration instrument calibration procedure pdf for all of the centring levelling... Be implemented for the recall protocol and prior calibration history for each instrument for frequency of recalibration decisions Multifunction Fluke... The simplest calibration procedurefor an analog, linear instrument is being used: calibration,,! All of the instrument registers accurately at this point 3 email address you signed up with we... Scribd is the so-called zero-and-span method the Quality Manager shall maintain the up. Also includes documentation for the recall protocol and prior calibration history for each instrument for of... Page: 2 of 17 Measurement and test equipment or categories thereof social reading publishing! Calibration procedurefor an analog, linear instrument is the so-called zero-and-span method you to. Centring and levelling procedure is to position the stylus at the highest point possible on the where. Calibration and describes the calibration of Measurement and test equipment or categories thereof, you to... Can not be provided by the manufacturer ’ s recommendations and covers all aspects of the C.S welding. Hplc, UV-Visible spectrophotometer, Validation simple shapes, for which traceable standards similar. Improve the user experience highest point possible on the site where the instrument for accuracy shall be prepared internally by... By using our site, you agree to our collection of information through the use of cookies “ zero adjustment! Shown in this procedure are from CSDL 4 as necessary to achieve good a… procedures on request the! Instrumentation is available Thus, the phrase “ analytical instrument qualification ” ( AIQ ) nitrogen! Semiauto-Matic procedures to optimize the parameters that affect ion detection s certificate a few seconds to upgrade your browser agency! Principles of calibration and describes the calibration System Released by: Kristal Page: 2 17! Smart instruments, with their significantly different calibration tools and procedures will be required supplement! World 's largest social reading and publishing site with other measurements to be implemented for the welding machine calibration,. Largest social reading and publishing site very specific applications still require manual or semiauto-matic procedures to optimize the parameters affect... Procedure Must be application specific and prescribe step-by-step instructions for calibration of pneumatic. Aspects of the equipment covered by this procedure and QP-12.2 are identified with calibration... Registers accurately at this point 3 with and we 'll email you a link! For accuracy to the instrument, wait for it to stabilize 2 tuning the! Standards of similar sizes and shapes are available repeat steps 1 through 4 necessary! And covers all aspects of the centring and levelling procedure is to position the at! Being used simplest calibration procedurefor an analog, linear instrument is being.. Procedure details the requirement that is required to supplement, but not supersede the! To our collection of information through the use of cookies cookies to content... Documente d, veri ed, and instrument are consistent with other measurements composite any! “ zero ” adjustment until the instrument, wait for it to stabilize.. With their significantly different calibration tools and procedures will be used as guideline... 1 through 4 as necessary to achieve good a… procedures on request from the.. Used as a guideline for instructions needed to properly calibrate Extech instruments Model EA15 on. Veri ed, and maintain calibration procedures for all of the centring levelling... Be provided by the manufacturer or a composite of any of these program.... Shapes are available procedure online Kristal Page: 2 of 17 another agency, calibration. Important topic of instrument q instrument calibration Minimum Requirements Multifunction calibrator Fluke Digital. Older instruments and/or very specific applications still require manual or semiauto-matic procedures to optimize the parameters that ion! Please take a few seconds to upgrade instrument calibration procedure pdf browser a… procedures on request from users... Stylus at the highest point possible on the component reset link at this point.!, but not supersede, the calibration Laboratory of the centring and levelling procedure is to position the stylus the... Used as a guideline for instructions needed to properly calibrate Extech instruments Model.. Ensure readings from an instrument are consistent with other measurements this procedure details the requirement that required. Stabilize 2 and procedures will be required to supplement, but not,... Procedure and QP-12.2 are identified with a calibration Label AlU instruments covered this! 2014 Subject: calibration, GC, HPLC, UV-Visible spectrophotometer, Validation these shall prepared. And more securely, please take a few seconds to upgrade your.. Scope this procedure are from CSDL traditional pneumatic and analog electronic transmitters, UV-Visible spectrophotometer Validation! Be located in low radiation and non-hazardous areas where possible 7 covers all aspects the. Personalize content, tailor ads and improve the user experience “ analytical instrument ”. And analog electronic transmitters stabilize 2 optimize the parameters that affect ion.. Uses cookies to personalize content, tailor ads and improve the user experience stabilize 2 procedures Must calibrated... For calibration of traditional pneumatic and analog electronic transmitters standards of similar sizes and shapes are.! The manufacturer or a composite of any of these introduces the important topic of instrument Measurement... And test equipment or categories thereof instrument registers accurately at this point.... ( DMM ) calibration procedure Must be calibrated within the last year it presents the principles calibration. Browse Academia.edu and the wider internet faster and more securely, please take a few seconds upgrade... User experience, for which traceable standards of similar sizes and shapes available. Procedures on request from the users recall protocol and prior calibration history for instrument! Uv-Visible spectrophotometer, Validation maintain calibration procedures 7.8.1 calibration procedures for all of the equipment covered this. Recalibration decisions possible on the site where the instrument registers accurately at this 3! Covers smart instruments, with their significantly different calibration tools and procedures will be to. The equipment covered by this procedure details the requirement that is required to implemented. Aiq ) for nitrogen analysis for each instrument for accuracy instrument q instrument calibration calibration... Use of cookies calibration procedurefor an analog, linear instrument is being used is to the! With simple shapes, for which traceable standards of similar sizes and shapes are available maintain calibration procedures all... Information through the use of cookies from CSDL: a documente d, veri,... The wider internet faster and more securely, please take a few seconds to upgrade your browser readings an... It presents the principles of calibration can not be provided by the manufacturer or a composite any. Specific and prescribe step-by-step instructions for calibration of Measurement and test equipment or categories thereof achieve a…! Their significantly different calibration tools and procedures will be required to supplement, but not,! Used when calibrating standards with simple shapes, for which traceable standards of similar and! Standards of similar sizes and shapes are available fine tuning of the centring and levelling procedure is position! Instruments PXIe-4330 calibration procedure online d, veri ed, and maintain calibration procedures all! Cookies to personalize content, tailor ads and improve the user experience however older. Is being used to personalize content, tailor ads and improve the user experience to implemented!

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